Collect. Czech. Chem. Commun.
1994, 59, 2663-2676
https://doi.org/10.1135/cccc19942663
Hugershoff Reaction of N-1- or N-2-Naphthoyl-N'-monosubstituted and N',N'-Disubstituted Thiourea Derivatives
Milan Dzurilla, Peter Kutschy, Ján Imrich and Stanislav Brtoš
Department of Organic Chemistry, P. J. Šafárik University, 041 67 Košice, Slovak Republic
Abstract
Hugershoff reaction of N-1- or N-2-naphthoyl-N'-monosubstituted and N',N'-disubstituted thiourea derivatives, prepared by the reaction of 1-naphthoyl or 2-naphthoyl isothiocyanate with primary or secondary amines, was studied. Depending on substituents the corresponding urea or benzothiazole derivatives were obtained as reaction products. Their structure was determined on the basis of infrared, 1H and 13C NMR and mass spectra.